HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21195152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21195145 | HCID 21195145 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21195152 | HCID 21195152 | — |
Reaction Steps
To 1 g of 4′-(4-methoxyphenyl)-2,2′:6′2″-terpyridine-6-carboxylic acid is added a solution of 1 mL of thionyl chloride in 25 mL of methylene chloride. The reaction mixture is heated gently for 1 hour, and the solvent and excess thionyl chloride are removed under reduced pressure. The crude product is triturated with anhydrous heptane and isolated by filtration under nitrogen.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248870B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-8334bc69f48b4e4297de34eea8e68e58 |
| Source note | uspto-grants-2001_06 |