Methanol → HCID 178496795, compound

Participants

Reaction Steps

0.95 g (5.00 mmol) of methyl N′-dimethoxymethylenehydrazinecarboxylate (85% pure) was admixed with 3.57 g of a 44% strength solution of methylamine (50 mmol) in methanol, and the mixture was stirred at room temperature for 3 days. Work-up and removal of the solvent gave 0.85 g (76%) of methyl N′-(methoxymethylaminomethylene)hydrazinecarboxylate in the form of an oil.

Provenance & Evidence