Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1068151Generated: October 30, 2026

Ammonium formate → HCID 15549372, compound

https://huagongshe.com/reaction/1068151

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmonium formateHCID 2723923—
ReactantHCID 9905121HCID 9905121—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 15549372HCID 1554937282.2%

Reaction Steps

To a solution of 100 mg of 3-(1-benzyl-piperidin-4-yl)-3-H-quinazolin-4-one (from Step B) in 6 mL of MeOH was added 100 mg of ammonium formate followed by 100 mg of 10% palladium on carbon. After refluxing for 5 hours, the mixture was filtered through celite. Concentration under reduced pressure afforded 59 mg of the title compound as a foamy solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06248755B1
Source datasetuspto-grants-2001_06
ORD IDord-d6e425786d30406596dc48a821cc58de
Source noteuspto-grants-2001_06