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HRID1068184

反应详情

EQUATION

反应方程式

HRID 1068184 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)C(C(C)=O)c1ccccc1
HCID95389

Ethyl 3-oxo-2-phenylbutanoate

C12H14O3

结构：NNC1CCN(Cc2ccccc2)CC1
HCID416192

未命名化合物

PRODUCTS

生成物

1
结构：Cc1[nH]n(C2CCN(Cc3ccccc3)CC2)c(=O)c1-c1ccccc1
HCID21193008

未命名化合物

收率 77.7%

PROCEDURE

实验过程

When 1.4 g of 1-benzyl-4-hydrazinopiperidine and 2.0 g of ethyl 2-phenylacetoacetate were used in the procedure of Example 124, Step A, there was obtained 1.84 g of 1-benzyl-4-(5-methyl-4-phenyl-1H-pyrazol-3(2H)-on-2-yl)-piperidine. ESI-MS 348.2 (M+H); HPLC A: 1.95 min.