Hydrochloric Acid → HCID 178499561, compound

HRID 1068401Notes

Reaction equation

HRID 1068401 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (400 g, 24.6 mmol) in methanol (100 ml) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature for 18 hrs. The solvent was evaporated in vacuo to afford the title compound as a white solid.

Workup

  1. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-13bc8931db4647eca2aea7b77f94e79c
Source dataset
uspto-grants-2001_06
Patent number
US06248756B1

Reaction notes

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