HRID1068407

反应详情

EQUATION

反应方程式

HRID 1068407 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 1-(4 cyanobenzyl)-5-nitro-1H-imidazole (100 mg, 0.438 mmol) and 10% palladium on carbon was hydrogenated in the presence of 1 equivalent of HCl under Parr conditions for 1 hr. Removal of the catalyst by filtration and evaporation of solvent in vacuo afforded the title compound.

WORKUP

后处理

  1. customRemoval of the catalyst
  2. filtrationby filtration and evaporation of solvent in vacuo