HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[2-{1-(Triphenylmethyl)-4-imidazolyl}ethenyl]-1-phenylpiperidine → 4-[2-{1-(Triphenylmethyl)-4-imidazolyl}ethyl]-1-phenylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[2-{1-(Triphenylmethyl)-4-imidazolyl}ethenyl]-1-phenylpiperidine | HCID 70243200 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | 4-[2-{1-(Triphenylmethyl)-4-imidazolyl}ethyl]-1-phenylpiperidine | HCID 21193360 | — |
Reaction Steps
The product from Step E is dissolved in methanol and hydrogenated at 60 psi hydrogen with 10% palladium on carbon. When reaction is complete, the catalyst is filtered and the title compound obtained after evaporation of solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248756B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-86bf265c70d24327a721fe7e3912c0a6 |
| Source note | uspto-grants-2001_06 |