HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21193249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54052971 | HCID 54052971 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21193249 | HCID 21193249 | — |
Reaction Steps
A solution of methyl N-tert-butoxycarbonyl-4-(3-methyl-benzoyl)piperidine-4-carboxylate (77 mg) in ethyl acetate (10 mL) at 0° C. was saturated with hydrogen chloride gas. The resultant solution was stirred at 0° C. for 2.5 h. The product solution was concentrated under vacuum to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248756B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-491de4bf7fb2437d90b018f2b65a6bc9 |
| Source note | uspto-grants-2001_06 |