4-Fluorobenzyl chloride → HCID 11447904, compound

Participants

Reaction Steps

In the same apparatus and procedure as Example 1 above, 0.15 g (0.75 mmol) of tri-n-butylphosphine, 1.08 g (7.5 mmol) of 4-fluorobenzyl chloride, and 5.08 g (37.5 mmol) of trichlorosilane were reacted at 150° C. for 2 hrs. The resulting mixture was distilled to give 1.6 g of (4-fluorobenzyl)trichlorosilane (bp; 56° C./13 mmHg, yield; 96%).

Provenance & Evidence