HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21190190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21190191 | HCID 21190191 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21190190 | HCID 21190190 | 100% |
Reaction Steps
To a solution of 3.21 g (8.87 mmol) of 4,5-dihydro-4-[4-(trifluoromethanesulfonamido)butan-1-yl]-3H-1,4,8b-triazaacenaphthylene in 10 ml of ethanol was added 2.0 ml of 12N HCl. The mixture was sufficiently blended. The solvent was distilled off under reduced pressure to leave 3.86 g of the desired compound (100%, colorless amorphous).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251905B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-928d63c940694c9cb56f88991a63772f |
| Source note | uspto-grants-2001_06 |