HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21190276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21190082 | HCID 21190082 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21190276 | HCID 21190276 | 100% |
Reaction Steps
In a solution consisting of 10 ml of ethanol and 1 ml of 12N HCl was dissolved 1.41 g (3.74 mmol) of 4,5-dihydro-2-methyl-4-[4-(trifluoromethanesulfonamido) butan-1-yl]-3H-1,4,8b-triazaacenaphthylene. The solvent was distilled off under reduced pressure to give the desired compound (100%, white amorphous).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251905B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-85040ec84441446a855206941cc9393e |
| Source note | uspto-grants-2001_06 |