Hydrochloric Acid → HCID 21190276, compound

HRID 1068698Notes

Reaction equation

HRID 1068698 reaction equation
[ClH:1].[CH3:2][C:3]1[N:4]=[C:5]2[N:14]3[C:9]([CH2:10][N:11]([CH2:15][CH2:16][CH2:17][CH2:18][NH:19][S:20]([C:23]([F:26])([F:25])[F:24])(=[O:22])=[O:21])[CH2:12][C:13]=13)=[CH:8][CH:7]=[CH:6]2>C(O)C>[ClH:1].[ClH:1].[CH3:2][C:3]1[N:4]=[C:5]2[N:14]3[C:9]([CH2:10][N:11]([CH2:15][CH2:16][CH2:17][CH2:18][NH:19][S:20]([C:23]([F:26])([F:25])[F:24])(=[O:21])=[O:22])[CH2:12][C:13]=13)=[CH:8][CH:7]=[CH:6]2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21190082HCID 21190082, compound

Product 1

HCID 21190276HCID 21190276, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a solution consisting of 10 ml of ethanol and 1 ml of 12N HCl was dissolved 1.41 g (3.74 mmol) of 4,5-dihydro-2-methyl-4-[4-(trifluoromethanesulfonamido) butan-1-yl]-3H-1,4,8b-triazaacenaphthylene. The solvent was distilled off under reduced pressure to give the desired compound (100%, white amorphous).

Workup

  1. distillationThe solvent was distilled off under reduced pressure

Sources & evidence

ORD record
ord-85040ec84441446a855206941cc9393e
Source dataset
uspto-grants-2001_06
Patent number
US06251905B1

Reaction notes

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