2-Naphthalenesulfonyl chloride → HCID 730263, compound

HRID 1068857Notes

Reaction equation

HRID 1068857 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([OH:7])=[O:6].[CH:11]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH:14]=[CH:13][C:12]=1[S:21](Cl)(=[O:23])=[O:22]>>[CH:11]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH:14]=[CH:13][C:12]=1[S:21]([NH:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([OH:7])=[O:6])(=[O:22])=[O:23]

Participants

3

Reactant 2

HCID 71252-Naphthalenesulfonyl chlorideHCID 74193-Aminobenzoic Acid

Product 1

HCID 730263HCID 730263, compoundYield 90.4%

Procedure

5 g (35.5 mmol) of 3-aminobenzoic acid and 8.3 g (36.5 mmol) of 2-naphthylsulfonyl chloride were reacted by the method of procedure 4b, affording 10.5 g (89%) of the product.

Sources & evidence

ORD record
ord-7eecd99f8fd5449987ed2b5df20c69ed
Source dataset
uspto-grants-2001_06
Patent number
US06251917B1

Reaction notes

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