3,4-Dimethoxystyrene → HCID 21190809, compound

HRID 1068861Notes

Reaction equation

HRID 1068861 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][C:10]=1[O:11][CH3:12])[CH:6]=[CH2:7].Br[C:14]1[CH:24]=[CH:23][CH:22]=[CH:21][C:15]=1[C:16]([O:18][CH2:19][CH3:20])=[O:17]>CN(C)C=O>[CH3:1][O:2][C:3]1[CH:4]=[C:5](/[CH:6]=[CH:7]/[C:21]2[CH:22]=[CH:23][CH:24]=[CH:14][C:15]=2[C:16]([O:18][CH2:19][CH3:20])=[O:17])[CH:8]=[CH:9][C:10]=1[O:11][CH3:12]

Participants

4

Reactant 2

HCID 614003,4-DimethoxystyreneHCID 80186Ethyl 2-bromobenzoate

Product 1

HCID 21190809HCID 21190809, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

5 g (30.5 mmol) of 3,4-dimethoxystyrene were reacted with ethyl 2-bromobenzoate in dimethylformamide at 120° C. by the method of procedure 31a. 1.2 g (4%) [sic] of the product were obtained.

Workup

  1. custom1.2 g (4%) [sic] of the product were obtained

Sources & evidence

ORD record
ord-e1844e6d7e864cdeadc817f9d5b06414
Source dataset
uspto-grants-2001_06
Patent number
US06251917B1

Reaction notes

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