2-Naphthalenesulfonyl chloride → HCID 2577221, compound

HRID 1068868Notes

Reaction equation

HRID 1068868 reaction equation
[NH2:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.[CH:12]1[C:21]2[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=2)[CH:15]=[CH:14][C:13]=1[S:22](Cl)(=[O:24])=[O:23]>>[CH:12]1[C:21]2[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=2)[CH:15]=[CH:14][C:13]=1[S:22]([NH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([OH:9])=[O:8])=[CH:10][CH:11]=1)(=[O:23])=[O:24]

Participants

3

Reactant 2

HCID 71252-Naphthalenesulfonyl chlorideHCID 655264-(Aminomethyl)Benzoic Acid

Product 1

HCID 2577221HCID 2577221, compoundYield 72%

Procedure

3.8 g (25 mmol) of 4-(aminomethyl)benzoic acid were reacted with 2-naphthalenesulfonyl chloride by the method of procedure 4b, affording 6.1 g (72%) of the product.

Sources & evidence

ORD record
ord-62ff6a8b74114f1fac98ecae9ed32bc6
Source dataset
uspto-grants-2001_06
Patent number
US06251917B1

Reaction notes

Loading…