HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21190629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Chloro-4-fluoroaniline | HCID 9708 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21190629 | HCID 21190629 | — |
Reaction Steps
1.75 g (12 mmol) of 3-chloro-4-fluoroaniline are dissolved in 20 ml of methanol, and 3 ml (12 mmol) of HCl (4.0N) are added. Concentration and drying (40° C., HV) yield 3-chloro-4-fluoro-aniline hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251911B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-661d5950023c43f3959314c513349884 |
| Source note | uspto-grants-2001_06 |