Hydrochloric Acid → HCID 21190629, compound

HRID 1068891Notes

Reaction equation

HRID 1068891 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[F:9])[NH2:5].Cl>CO>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[F:9])[NH2:5]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 97083-Chloro-4-fluoroaniline

Product 1

HCID 21190629HCID 21190629, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.75 g (12 mmol) of 3-chloro-4-fluoroaniline are dissolved in 20 ml of methanol, and 3 ml (12 mmol) of HCl (4.0N) are added. Concentration and drying (40° C., HV) yield 3-chloro-4-fluoro-aniline hydrochloride.

Workup

  1. concentrationConcentration
  2. customdrying (40° C., HV)

Sources & evidence

ORD record
ord-661d5950023c43f3959314c513349884
Source dataset
uspto-grants-2001_06
Patent number
US06251911B1

Reaction notes

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