Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Aminopyridine | HCID 10009 | — |
| Reactant | 2-(Bis(methylsulfanyl)methylidene)propanedinitrile | HCID 99229 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 1704483 | HCID 1704483 | — |
Reaction Steps
A mixture of 11 g (64.6 mmol) of 3,3-bis-methylmercapto-2-cyano-acrylonitrile, 6 g (63.75 mmol) of 3-amino-pyridine and 50 ml of toluene is stirred at 60° C. for 18 hours. Filtration of the reaction mixture while still warm and washing of the filter residue with toluene yield 2-cyano-3-methylmercapto-3-(3-pyridylamino)-acrylonitrile; m.p. 180-181° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06251911B1 |
|---|
| Source dataset | uspto-grants-2001_06 |
|---|
| ORD ID | ord-eeaca6f19d884ffda3d65664fabcc352 |
|---|
| Source note | uspto-grants-2001_06 |
|---|
