HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 77750336, compound → HCID 77750205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 77750336 | HCID 77750336 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 77750205 | HCID 77750205 | 64.7% |
Reaction Steps
A solution of the product of Example 53, step (c) (0.2 g) and triisopropylbenzenesulphonylhydrazide (0.3 g) in tetrahydrofuran (10 ml) was heated at 70° C. for 4 hours. The mixture was then purified (SiO2, ethyl acetate as eluant) to afford the title compound (0.13 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251910B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-b5c86ab76f284c02b6cecf963cc6c111 |
| Source note | uspto-grants-2001_06 |