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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1069036Generated: October 30, 2026

HCID 77750336, compound → HCID 77750205, compound

https://huagongshe.com/reaction/1069036

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 77750336HCID 77750336—
SolventTetrahydrofuranHCID 8028—
ProductHCID 77750205HCID 7775020564.7%

Reaction Steps

A solution of the product of Example 53, step (c) (0.2 g) and triisopropylbenzenesulphonylhydrazide (0.3 g) in tetrahydrofuran (10 ml) was heated at 70° C. for 4 hours. The mixture was then purified (SiO2, ethyl acetate as eluant) to afford the title compound (0.13 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06251910B1
Source datasetuspto-grants-2001_06
ORD IDord-b5c86ab76f284c02b6cecf963cc6c111
Source noteuspto-grants-2001_06