HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanethiol → HCID 77750276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanethiol | HCID 8012 | — |
| Reactant | HCID 77750102 | HCID 77750102 | — |
| Product | HCID 77750276 | HCID 77750276 | — |
Reaction Steps
Prepared by the method of Example 4, step (b) using the product of Example 110, step a) and butanethiol then deprotected using the method of Example 1, step (b). Purification (HPLC, Novapak® C18 column, 0.1% aqueous ammonium acetate:acetonitrile, isocratic elution 45% MeCN over 30 minutes) afforded the title compound (210 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251910B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-a45c08cb38604dd78e284a9340af3990 |
| Source note | uspto-grants-2001_06 |