HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 21191269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | HCID 21191249 | HCID 21191249 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21191269 | HCID 21191269 | — |
Reaction Steps
Under a nitrogen atmosphere in a three-neck round bottom flask 3-[(4-acetyl-3-hydroxy-2-propylphenoxy)methyl]benzaldehyde (0.73 g, 2.34 mmol), rhodanine (0.34 g, 2.55 mmol), sodium acetate (0.23 g, 2.80 mmol) and acetic acid (20 ml) were combined and then heated to reflux. The reaction mixture was allowed to reflux. The progress of the reaction was monitored by thin layer chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251928B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-613003df04e74d578ef94ae4d3448e0c |
| Source note | uspto-grants-2001_06 |