HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 86752511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | HCID 21191275 | HCID 21191275 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86752511 | HCID 86752511 | — |
Reaction Steps
Under a nitrogen atmosphere in a round bottom flask 4-[(3-phenylphenyl)methoxy]benzaldehyde (3.2 g, 10 mmol) was dissolved in acetic acid. To this solution, while stirring, were added sodium acetate (2.87 g, 35 mmol) and rhodanine (1.33 g, 10 mmol). This mixture was heated to reflux and maintained at this temperature. The progress of this reaction was monitored by thin layer chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251928B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-f3071acb18a34952870f4adc7a765a78 |
| Source note | uspto-grants-2001_06 |