HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 86752516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | 4-[[2-(Trifluoromethyl)phenyl]methoxy]benzaldehyde | HCID 21191284 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86752516 | HCID 86752516 | — |
Reaction Steps
Under a nitrogen atmosphere in a round bottom flask 4-[(2-trifluoromethylphenyl)methoxy]benzaldehyde (2.98 g, 10.63 mmol), sodium acetate (3.05 g, 37.2 mmol), and rhodanine (1.42 g, 10.7 mmol) were dissolved in 53 ml of acetic acid. The reaction solution was then heated to reflux and maintained at this temperature for about three days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06251928B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-4a5b2821e7f440e09b333fd7276c3244 |
| Source note | uspto-grants-2001_06 |