HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Bromomethyl)thiophene → HCID 86757061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Bromomethyl)thiophene | HCID 520703 | — |
| Reactant | Methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate | HCID 11079278 | — |
| Product | HCID 86757061 | HCID 86757061 | 84% |
Reaction Steps
This compound is prepared from 5 g (13.4 mmol) of methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate and 2.9 g (16.4 mmol) of 3-bromomethyl-thiophene according to the method described in 1.5. 3.5 g of product are obtained in the form of yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252082B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-52154b046f5e4bb49c64002c3b9a5864 |
| Source note | uspto-grants-2001_06 |