HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Bromomethyl)-4-(1,1-dimethylethyl)benzene → HCID 70186997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Bromomethyl)-4-(1,1-dimethylethyl)benzene | HCID 87836 | — |
| Reactant | Methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate | HCID 11079278 | — |
| Product | HCID 70186997 | HCID 70186997 | 72.9% |
Reaction Steps
This compound is prepared from 5 g (13.4 mmol) of methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate and 4.54 g (20 mmol) of 4-(1,1-dimethylethyl)phenylmethyl bromide according to the method described in 1.5. 3.5 g of product are obtained in the form of yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252082B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-cea58c8bff1b45dca0e0f085486f4d2d |
| Source note | uspto-grants-2001_06 |