4-(Bromomethyl)benzonitrile → HCID 86757064, compound

HRID 1069434Notes

Reaction equation

HRID 1069434 reaction equation
[CH3:1][C:2]1[N:7]([CH2:8][C:9]([O:11][CH3:12])=[O:10])[C:6](=[O:13])[C:5]([N+:14]([O-:16])=[O:15])=[C:4](OS(C(F)(F)F)(=O)=O)[CH:3]=1.[C:25]([C:27]1[CH:32]=[CH:31][C:30]([CH2:33]Br)=[CH:29][CH:28]=1)#[N:26]>>[C:25]([C:27]1[CH:32]=[CH:31][C:30]([CH2:33][C:4]2[CH:3]=[C:2]([CH3:1])[N:7]([CH2:8][C:9]([O:11][CH3:12])=[O:10])[C:6](=[O:13])[C:5]=2[N+:14]([O-:16])=[O:15])=[CH:29][CH:28]=1)#[N:26]

Participants

3

Reactant 2

HCID 869964-(Bromomethyl)benzonitrileHCID 11079278Methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate

Product 1

HCID 86757064HCID 86757064, compound

Procedure

This compound is prepared from 15.3 g (40.9 mmol) of methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate and 10 g (51 mmol) of (4-cyanophenyl)methyl bromide according to the method described in Example 1.5.

Sources & evidence

ORD record
ord-b2faa3ae3ad74d708ee71403981c1bde
Source dataset
uspto-grants-2001_06
Patent number
US06252082B1

Reaction notes

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