HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 86757066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate | HCID 11079278 | — |
| Reactant | HCID 21191804 | HCID 21191804 | — |
| Product | HCID 86757066 | HCID 86757066 | — |
Reaction Steps
It is prepared from 7.3 g (27 mmol) of N-acetyl-N-[4-(bromomethyl)phenyl]acetamide and 4 g (13.4 mmol) of methyl 6-methyl-3-nitro-2-oxo-4-[[(trifluoromethyl)sulphonyl]oxy]-1,2-dihydropyridine-1-acetate. The crude product is treated with ammonia.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252082B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-2bab55dab9524b6e9771662d638c9537 |
| Source note | uspto-grants-2001_06 |