Benzyl chloroformate → HCID 70187007, compound

HRID 1069444Notes

Reaction equation

HRID 1069444 reaction equation
[NH2:1][C:2]1[C:3](=[O:21])[N:4]([CH2:16][C:17]([O:19][CH3:20])=[O:18])[C:5]([CH3:15])=[CH:6][C:7]=1[S:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.ClC(O[CH2:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)=O>>[CH3:15][C:5]1[N:4]([CH2:16][C:17]([O:19][CH3:20])=[O:18])[C:3](=[O:21])[C:2]([NH:1][C:17]([O:19][CH2:20][CH2:26][C:27]2[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=2)=[O:18])=[C:7]([S:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:6]=1

Participants

3

Reactant 2

HCID 10387Benzyl chloroformateHCID 70186511HCID 70186511, compound

Product 1

HCID 70187007HCID 70187007, compound

Procedure

1.7 g (5.6 mmol) of methyl 3-amino-6-methyl-2-oxo-4-(phenylthio)-1,2-dihydropyridine-1-acetate are treated with 1.2 ml (8.4 mmol) of phenylmethyl chloroformate under the conditions described in Example 3.

Sources & evidence

ORD record
ord-b7841c361d134ba3a2153615c0471476
Source dataset
uspto-grants-2001_06
Patent number
US06252082B1

Reaction notes

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