HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-hexyl-5-methoxy-2-methyl-1H-indole-3-acetamide → HCID 21191844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-hexyl-5-methoxy-2-methyl-1H-indole-3-acetamide | HCID 21191895 | — |
| Reactant | Boron tribromide dichloromethane | HCID 22277759 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21191844 | HCID 21191844 | 101% |
Reaction Steps
A mixture of 1 mL of 1M BBr3/methylene chloride and 0.24 g (0.79 mmol) of 1-hexyl-5-methoxy-2-methyl-1H-indole-3-acetamide in 20 mL of methylene chloride as stirred for 16 hours, diluted with ethyl acetate and washed twice with water. The solution was dried (Na2SO4) and the solvent removed at reduced pressure to give 0.23 g of crude 1-hexyl-5-hydroxy-2-methyl-1H-indole-3-acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06252084B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-ad8f6a5edda346ee995b5c5daa2d1faa |
| Source note | uspto-grants-2001_06 |