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HRID10697

反应详情

EQUATION

反应方程式

HRID 10697 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccc(C(=O)O)cc1
HCID11470

4-Acetylbenzoic acid

C9H8O3

结构：COc1cc(OC)c(-c2nn[nH]n2)cc1C=O
HCID21981081

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(OC)c(-c2nn[nH]n2)cc1/C=C/C(=O)c1ccc(C(=O)O)cc1
HCID10126430

未命名化合物

收率 19%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

The title compound was prepared by condensing 2,4-dimethoxy-5-(2H-tetrazol-5-yl)-benzaldehyde (Ex-75A) and 4-acetylbenzoic acid in a similar manner as described in Ex-3. Yellow solid, 19% yield, mp 218° C. (dec). 1H-NMR (DMSO-d6) δ 8.58 (s, 1H), 8.20 (d, 2H), 8.03 (m, 3H), 7.85 (d, 1H), 6.90 (s, 1H), 4.04 (s, 3H), 4.02 (s, 3H). MS m/z=422 ([M+CH3CN+H]+, 100%). HRMS m/z: calc. 381.1199, found 381.1184.