HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → 3-[3-(2-pyridinyl)-1H-1,2,4-triazol-5-yl]propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | Picolinimidohydrazide | HCID 70493 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | 3-[3-(2-pyridinyl)-1H-1,2,4-triazol-5-yl]propanoic acid | HCID 22396183 | — |
Reaction Steps
2-Pyridinecarbohydrazonamide (0.136 g) and dihydro-2,5-furandione (0.100 g) in 1 ml of dimethylacetamide was heated for 10 times 30 seconds in a CEM MARS 5 microwave at 100% of 300 W under nitrogen to leave 3-[3-(2-pyridinyl)-1H-1,2,4-triazol-5-yl]propanoic acid in 1 ml of dimethylacetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903085B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-8f4d74c2f09646599c8c7db03cb7bd07 |
| Source note | uspto-grants-2005_06 |