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HRID1070504

反应详情

EQUATION

反应方程式

HRID 1070504 的结构方程式

REACTANTS

反应物

2
结构：O=C1CCC(=O)O1
HCID7922

Succinic anhydride

C4H4O3

结构：NN=C(N)c1ccccn1
HCID70493

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)CCc1nc(-c2ccccn2)n[nH]1
HCID22396183

5-(2-Pyridinyl)-1H-1,2,4-triazole-3-propanoic acid

C10H10N4O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

2 次

PROCEDURE

实验过程

2-Pyridinecarbohydrazonamide (0.136 g) and dihydro-2,5-furandione (0.100 g) in 1 ml of dimethylacetamide was heated for 10 times 30 seconds in a CEM MARS 5 microwave at 100% of 300 W under nitrogen to leave 3-[3-(2-pyridinyl)-1H-1,2,4-triazol-5-yl]propanoic acid in 1 ml of dimethylacetamide.