HCID 22397334, compound → HCID 22397314, compound

HRID 1070562Notes

Reaction equation

HRID 1070562 reaction equation
[C:1]([O:5][C:6]([N:8]([CH:14]1[CH2:17][CH2:16][CH2:15]1)[CH2:9][CH2:10][C:11]([O-])=[O:12])=[O:7])([CH3:4])([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCCC>[C:1]([O:5][C:6]([N:8]([CH:14]1[CH2:15][CH2:16][CH2:17]1)[CH2:9][CH2:10][CH2:11][OH:12])=[O:7])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 1

HCID 22397334HCID 22397334, compound

Product 1

HCID 22397314HCID 22397314, compound

Reagents, catalysts & solvents 1

HCID 21899848Ethylacetate heptaneSolvent

Procedure

This compound was prepared from N-tertbutoxycarbonyl-3-cyclobutylamino-propanoate (4a, 1.71 9, 6.3 mmol) using the procedure described in Example 2b. Yield: 0.94 g (65%). ESI-MS: 230.2 (M+H)+. 252.3 (M+Na)+, 174.2 (M+H—C4H8)+. Rf (silica gel; ethyl acetate/heptane, 1:4, v/v): 0.37.

Sources & evidence

ORD record
ord-8c9cf30f68f64e8b916c7a6527aae8c0
Source dataset
uspto-grants-2005_06
Patent number
US06903107B1

Reaction notes

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