HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22397334, compound → HCID 22397314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22397334 | HCID 22397334 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 22397314 | HCID 22397314 | — |
Reaction Steps
This compound was prepared from N-tertbutoxycarbonyl-3-cyclobutylamino-propanoate (4a, 1.71 9, 6.3 mmol) using the procedure described in Example 2b. Yield: 0.94 g (65%). ESI-MS: 230.2 (M+H)+. 252.3 (M+Na)+, 174.2 (M+H—C4H8)+. Rf (silica gel; ethyl acetate/heptane, 1:4, v/v): 0.37.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903107B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-8c9cf30f68f64e8b916c7a6527aae8c0 |
| Source note | uspto-grants-2005_06 |