HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → HCID 22397321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | tert-Butyl Formate | HCID 61207 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 22397321 | HCID 22397321 | — |
Reaction Steps
The title compound was prepared from ethyl acrylate (1.09 ml, 10 mmol) and cyclopropylamine (0.69 ml, 10 mmol) according to Example 2a. Yield: 2.06 g (80%). ESI-MS: 258.2 (M+H)+, 202.2 (M+H—C4H8)+, 158.2 (M+H-Boc)+. Rf (silica gel; ethyl acetate/heptane, 1:4, v/v): 0.38.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903107B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-e8a5361276bc4c369e16d7482d0da95a |
| Source note | uspto-grants-2005_06 |