HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 22397381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 2,3-Dimethoxynaphthalene | HCID 604708 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22397381 | HCID 22397381 | — |
Reaction Steps
Aluminum chloride (16.0 g) was added to a solution of 2,3-dimethoxynaphthalene (18.0 g) and benzoylchloride (12.0 g) in cold methylene chloride (400 ml) and the solution was stirred overnight. After treatment with cold water the phases were separated and the methylene chloride phase washed with 1 M sodium hydroxide. The product was triturated with warm ether. Yield: 7 g, melting point 124-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903114B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-97200d0443444a6287e67301b6d87977 |
| Source note | uspto-grants-2005_06 |