HuagongsheHuagongshe Chemistry Print Report · For research reference only
Palmitoyl chloride → HCID 22397410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Palmitoyl chloride | HCID 8206 | — |
| Reactant | 2,3-Dimethoxynaphthalene | HCID 604708 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22397410 | HCID 22397410 | — |
Reaction Steps
The solution of 2,3-dimethoxynaphthalene (1.9 g), palmitoyl chloride (3.2 ml) and aluminium chloride (1.5 g) in methylene chloride (40 ml) was stirred at ambient temperature overnight. The reaction mixture was worked up as described in example 4(a). The crude product was recrystallized from ethyl acetate-heptane. Yield 2.0 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903114B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-47e36acc28a4494598d8aa5e04bc0cdd |
| Source note | uspto-grants-2005_06 |