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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1070669Generated: November 1, 2026

Palmitoyl chloride → HCID 22397410, compound

https://huagongshe.com/reaction/1070669

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPalmitoyl chlorideHCID 8206—
Reactant2,3-DimethoxynaphthaleneHCID 604708—
ReactantAluminum(III) ChlorideHCID 6451240—
SolventDichloromethaneHCID 6344—
ProductHCID 22397410HCID 22397410—

Reaction Steps

The solution of 2,3-dimethoxynaphthalene (1.9 g), palmitoyl chloride (3.2 ml) and aluminium chloride (1.5 g) in methylene chloride (40 ml) was stirred at ambient temperature overnight. The reaction mixture was worked up as described in example 4(a). The crude product was recrystallized from ethyl acetate-heptane. Yield 2.0 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06903114B2
Source datasetuspto-grants-2005_06
ORD IDord-47e36acc28a4494598d8aa5e04bc0cdd
Source noteuspto-grants-2005_06