HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 868381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2,3-Dihydroxynaphthalene | HCID 7091 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 868381 | HCID 868381 | — |
Reaction Steps
Acetylchloride (0.71 ml) was added to a solution of 2,3-dihydroxynaphthalene (1.6 g) and pyridine (0.81 ml) in ethyl acetate (20 ml) at 0° C. The mixture was stirred for few hours at room temperature and then washed with water, dried and evaporated to dryness. The crude product was recrystallized from ether. Yield: 0.52 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903114B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-593b849f30a1492b9782085ca83d665f |
| Source note | uspto-grants-2005_06 |