HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthalenesulfonyl chloride → HCID 77692401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthalenesulfonyl chloride | HCID 7125 | — |
| Reactant | HCID 57010858 | HCID 57010858 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 77692401 | HCID 77692401 | — |
Reaction Steps
Batch size: 8.0 g (22.6 mmol) N-(2-(piperazin-1-yl)-ethyl]-3-pyridin-3-yl-acrylamide.trihydrochloride (substance 317 as a trihydrochloride), 13 ml (92.7 mmol) TEA and 5.6 g (24.9 mmol) naphthalin-2-sulfonic acid chloride in 180 ml absolute dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903118B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-05e5e0aef4e34f259bdab9b825029ad7 |
| Source note | uspto-grants-2005_06 |