HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 4-[1,1′-Biphenyl]-2-yl-1-piperazinebutanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 22397693 | HCID 22397693 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-[1,1′-Biphenyl]-2-yl-1-piperazinebutanamine | HCID 22397614 | — |
Reaction Steps
Batch size: 20.8 g (47.3 mol) 2-[4-(4-biphenyl-2-yl-piper-azin-1-yl)-butyl]-isoindolin-1,3-dione and 4.6 ml (94.6 mmol) hydrazine-hydrate in 185 ml ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06903118B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-bbf3d6618f4d4922ae652a6342194fe8 |
| Source note | uspto-grants-2005_06 |