HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178488143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 178488115 | HCID 178488115 | — |
| Product | HCID 178488143 | HCID 178488143 | — |
Reaction Steps
The title compound was prepared by the method of Example 3 using 2.00 g of the title product of Example 35 instead of the title product of Example 2. Trituration with diethylether gave 1.58 g of the title compound: m.p. 142-144° C. Analysis. Calc'd. for C16H17N3O2S: C, 60.93; H, 5.43; N, 13.32; S, 10.17. Found: C, 60.60; H, 5.42; N, 12.83; S, 9.86.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06906078B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-30da31eeefa24360ac69215e2cffd2be |
| Source note | uspto-grants-2005_06 |