Water → HCID 22394088, compound

HRID 1071565Notes

Reaction equation

HRID 1071565 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]1[CH:13]=[CH:14][C:15]([NH2:18])=[N:16][CH:17]=1.[OH2:19]>>[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:13]=[CH:14][C:15]([NH2:18])=[N:16][CH:17]=1)=[O:19]

Participants

3

Reactant 2

HCID 962WaterHCID 22394140HCID 22394140, compound

Product 1

HCID 22394088HCID 22394088, compound

Procedure

The title compound was prepared by the method of Example 85 using 1.0 g (3.9 mmole) of 5-[(1H-benzimidazol-2-ylthio)methyl]-2-pyridinamine (see Example 110) instead of 6-[(1H-benzimidazol-2-ylthio)methyl]-2-pyridinamine. Structure assignment was supported by the nmr and infrared spectra and by elemental analysis. Analysis. Calc'd. for C13H12N4SO*¼ H2O: C, 56.40; H, 4.55; N, 20.24; S, 11.58. Found: C, 56.35; H, 4.46; N, 20.25; S, 11.66.

Sources & evidence

ORD record
ord-3edf33224a2942539f2e71a3f3bb8a8b
Source dataset
uspto-grants-2005_06
Patent number
US06906078B2

Reaction notes

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