Aniline → Benzamide

Participants

Reaction Steps

The title compound was synthesized in the same manner as Example 1 using aniline (0.59 g, 6.4 mmol), CSI (0.67 mL, 7.7 mmol), and 3-amino-N-(3,4-difluoro-phenyl)-4-methoxy-benzamide (1.19 g, 4.3 mmol) to give 0.17 g of pure benzamide, N-(3,4-difluorophenyl)-4-methoxy-3-[[[[(phenylamino)carbonyl]amino]sulfonyl]amino]-. Microanalysis: C21H18F2N4O5S; calculated: C=52.94; H=3.81; N=11.76. found: C=52.70; H=4.04; N=11.51. MS: M++1=477 Da.

Provenance & Evidence