HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20800783, compound → HCID 11436230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20800783 | HCID 20800783 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11436230 | HCID 11436230 | 68.9% |
Reaction Steps
6.48 g of 1-benzyl-4-hydroxypropyl-1,2,5,6-tetrahydropyridine was dissolved in 60 ml of methanol, 88 mg of PtO2 was added, and atmosphere was replaced with hydrogen. After completion of the reaction, the mixture was filtered, and the filtrate was evaporated, to give 4.50 g (19.3 mmol, 68.9%) of the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06906072B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-e45f52124a1b4fef963713051a71173c |
| Source note | uspto-grants-2005_06 |