HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22393638, compound → HCID 22393627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22393638 | HCID 22393638 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22393627 | HCID 22393627 | 93.4% |
Reaction Steps
Ethyl 1-benzyl-4-(4-cyano-5-methyl-4-phenylhexyl)-2-piperazinecarboxylate (857 mg) was dissolved in ethanol (15 ml), and 770 mg of 10% Pd-C was added. After replacing the atmosphere with hydrogen, the mixture was stirred. After completion of the reaction, the solution was evaporated, to give 639 mg (93%) of the title compound as a crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06906072B1 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-190f5bf963a247468fa3d30ebb718bc4 |
| Source note | uspto-grants-2005_06 |