Diisopropylethylamine → HCID 69748139, compound

Participants

Reaction Steps

The hydrochloride salt of (1S,2R,3S)-1-(3,5-difluorobenzyl)-2,3-dihydroxyheptylamine (0.1 mmol) was reacted with 5-methyl-N,N-dipropyl-isophthalamic acid as described in method A (addition of an extra equivalent of DIEA to neutralize the amine salt) to give N1-[(1S,2R,3S)-1-(3,5-difluorobenzyl)-2,3-dihydroxy-octyl]-5-methyl-N3,N3-dipropyl-isophthalamide. MS (ESI+) for C29H40F2N2O4 m/z 540.9 (M+Na)+.

Provenance & Evidence