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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1071870Generated: November 2, 2026

Malononitrile → HCID 3773318, compound

https://huagongshe.com/reaction/1071870

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMalononitrileHCID 8010—
ReactantPiperidineHCID 8082—
Reactant3-Bromo-4,5-dimethoxybenzaldehydeHCID 81379—
SolventEthanolHCID 702—
ProductHCID 3773318HCID 3773318—

Reaction Steps

To a mixture of 5-bromoveratraldehyde (245 mg, 1 mmol) and malononitrile (66 mg, 1 mmol) in ethanol was added piperidine (0.1 ml, 1 mmol). The mixture was stirred at room temperature for 15 min to give the product 3,4-dimethoxy-5-bromobenzylidenemalononitrile as a yellow precipitate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06906203B1
Source datasetuspto-grants-2005_06
ORD IDord-724c91b018b448b0b40617583f3c1803
Source noteuspto-grants-2005_06