2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-

HRID 1071927Notes

Reaction equation

HRID 1071927 reaction equation
[CH3:1][C:2]1([CH3:9])[CH2:7][CH2:6][C:5](=[O:8])[CH:4]=[CH:3]1>CCCCC.[Pd]>[CH3:1][C:2]1([CH3:9])[CH2:7][CH2:6][C:5](=[O:8])[CH2:4][CH2:3]1

Participants

4

Reactant 1

HCID 1368392-Cyclohexen-1-one, 4,4-dimethyl-

Product 1

HCID 138166Cyclohexanone, 4,4-dimethyl-

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8003PentaneSolvent

Procedure

31.1 g of 4,4-dimethylcyclohex-2-enone in 100 ml of pentane are hydrogenated in an autoclave at a pressure of 5 bar in the presence of 1.6 g of 5% palladium on charcoal. The reaction mixture is filtered and the solvents are evaporated off under reduced pressure.

Workup

  1. filtrationThe reaction mixture is filtered
  2. customthe solvents are evaporated off under reduced pressure

Sources & evidence

ORD record
ord-e9e28ffba2814710813c096bdc522b3c
Source dataset
uspto-grants-2005_06
Patent number
US06908914B1

Reaction notes

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