HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22390615, compound → HCID 22390586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22390615 | HCID 22390615 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22390586 | HCID 22390586 | 92.6% |
Reaction Steps
N-(2-Methoxyethyl)-N-methyl-4-nitrobenzenesulphonamide (Method 10; 3.88 g) was reduced by hydrogenation in ethanol (100 ml) over 10% palladium on carbon (400 mg) at 3 bar pressure. The catalyst was removed by filtration and the volatiles evaporated to give the title compound (3.2 g). M/z: 245.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06908920B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-a01c1a0d0b7b4a668ebb52c37ea00c7f |
| Source note | uspto-grants-2005_06 |