HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Azidoethyl)benzamide → HCID 12666304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Azidoethyl)benzamide | HCID 22390689 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12666304 | HCID 12666304 | — |
Reaction Steps
Pd/C (11 mg, 0.11 mmol) was added to a solution of 4-(2-azidoethyl)benzamide (200 mg, 1.05 mmol) in EtOH (4 mL). A hydrogen balloon was placed over the reaction and it stirred for about four hours. The crude reaction was filtered through a pad of celite and concentrated to give 4-(2-aminoethyl)benzamide which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06908921B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-725358ff78ba474c82463404105b2143 |
| Source note | uspto-grants-2005_06 |